This system is an anti-corrosion manual sampling device. The parts in contact with the sampling medium are lined with PFA or Fluorine to achieve anti-corrosion purpose. The Teflon suction pipe matched with the insertion pipe (fluorine lined/ glass lined) is immersed below the medium liquid in the vessel to increase the stability of the process. The medium is sampled safely and quickly in the system by vacuuming.
装置步骤:Installation procedure:
1.将(拔出管)装置到澳门金狮
响应管口上紧固螺栓。
Install (the insertion pipe) on the corresponding nozzle of the reactor and fasten the bolts.
2.将取样体系下端(底座)与(隔阂阀1)拆分,将(底座)装置到(拔出管)上端。
Separate the lower end (base) of the sampling system from (diaphragm valve 1), and install (base) to the upper end of (insertion pipe).
3.将四氟外翻边(吸料管)装入(底座)内腔,四氟(吸料管)外翻边处于(阀座)密封面处符合。
Put the Teflon outer flanging (suction pipe) into the inner cavity of the (base), and the Teflon outer flange of (the suction pipe) is matched at the sealing surface of the (valve seat) .
4.将其他取样体系主体与其毗连紧固,保障(底座)密封处压紧、无泄露。
Connect and tighten the rest of the sampling system body to ensure that the sealing part of (base) is tight and without leakage.
备注:毗连装备小口管径时可取消底座部件。
Note: The base part can be canceled when connecting the device with small diameter pipe.
取样步骤:
Sampling procedure
1.取样前确认、查抄:Confirm and check before starting:
a:一切隔阂阀处于封闭状况。
All diaphragm valves are closed.
b:取样体系内、外无剩余物视镜无破坏。
There is no residue inside and outside the sampling system, and no damage to the sightglass.
c:真空体系与对应真空接口相连并确保密封无泄露。
The vacuum system is connected to the corresponding vacuum interface and ensure that the seal is leak-free.
d:反吹用0.2~0.3MPa氮气气源。
0.2~0.3 MPa nitrogen gas source is used for back blowing.
e:备用150/250mL硼硅玻璃取样瓶1支。
One spare 150/250 ml borosilicate glass sampling bottle is needed.
2.吸料:Suction:
Remove the (sampling bottle) and seal the bottle mouth - put in (spare sampling bottle) 。
e:翻开(隔阂阀1)——翻开(隔阂阀5)——翻开(隔阂阀3、隔阂阀4)。
Open (diaphragm valve 1)—Open (diaphragm valve 5)—Open (diaphragm valve 3 and diaphragm valve 4) .
a:翻开(隔阂阀1)。
Open (diaphragm valve 1) .
b:当令翻开(隔阂阀2)。
Open (diaphragm valve 2) in time.
c:察看(视镜)。浮球迟缓回升,布满视镜窗。
Observe (sightglass). The floater slowly rises and medium fills the sightglass window.
d:封闭(隔阂阀1、隔阂阀2)。
Close (diaphragm valve 1 and diaphragm valve 2) .
3.取样:Sampling:
a:翻开(隔阂阀3)。
Open (diaphragm valve 3)
b:翻开(隔阂阀4)。察看取样瓶量剂。
Open (diaphragm valve 4). Observe the dosage of the sampiing bottle.
c:封闭(隔阂阀3、隔阂阀4)。
Close (diaphragm valve 3 and diaphragm valve 4).
d:取下(取样瓶)密封瓶口——装入(备用取样瓶)。
氮气将体系内剩余物料反吹釜内。
Make nitrogen blow the residual medium in the system back into the vessel.
f:封闭(隔阂阀1、隔阂阀3、隔阂阀4、隔阂阀5)。
Close (diaphragm valve 1、diaphragm valve 3、diaphragm valve 4 and diaphragm valve 5) .
g:取祥竣事。
Sampling complete.
澳门金狮
带手动取样体系洗濯进程申明: Descript ionoftheCleani ngProcessoftheReactorwithManua15amp|ingSystern:
在停止全部澳门金狮
的洗濯进程中, 能够根据以上取样步骤描写停止取样体系外部洗濯、吹扫。
During the cleaning process of the whole reactor, the internal cleaning and purging of the sampling system can be carried out according to the above sampling steps.